Purdue University Graduate School
Hanhan_Dissertation_v06.pdf (23.91 MB)

Investigating damage in discontinuous fiber composites through coupled in-situ X-ray tomography experiments and simulations

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posted on 2020-04-29, 19:49 authored by Imad A HanhanImad A Hanhan

Composite materials have become widely used in engineering applications, in order to reduce the overall weight of structures while retaining their required strength. Due to their light weight, relatively high stiffness properties, and formability into complex shapes, discontinuous fiber composites are advantageous for producing small and medium size components. However, qualifying their mechanical properties can be expensive, and therefore there is a need to improve predictive capabilities to help reduce the overall cost of large scale testing. To address this challenge, a composite material consisting of discontinuous glass fibers in a polypropylene matrix is studied at the microstructural level through coupled experiments and simulations, in order to uncover the mechanisms that cause microvoids to initiate and progress, as well as certain fiber breakage events to occur, during macroscopic tension. Specifically, this work coupled in-situ X-ray micro computed tomography (μ-CT) experiments with a finite element simulation of the exact microstructure to enable a 3D study that tracked damage initiation and propagation, and computed the local stresses and strains in the microstructure. In order to have a comprehensive 3D understanding of the evolution of the microstructure, high fidelity characterization procedures were developed and applied to the μ-CT images in order to understand the exact morphology of the microstructure. To aid in this process, ModLayer - an interactive image processing tool - was created as a MATLAB executable, and the 3D microstructural feature detection techniques were compared to traditional destructive optical microscopy techniques. For damage initiation, this work showed how high hydrostatic stresses in the matrix can be used as a metric to explain and predict the exact locations of microvoid nucleation within the composite’s microstructure. From a damage propagation standpoint, matrix cracking - a mechanism that has been notably difficult to predict because of its apparent stochastic nature - was studied during damage propagation. The analysis revealed the role of shear stress in fiber mediated flat matrix cracking, and the role of hydrostatic stress in fiber-avoidance conoidal matrix cracking. Overall, a sub-fiber simulation and an in-situ experimental analysis provided the microstructural physical phenomena that govern certain damage initiation and progression mechanisms, further enabling the strength and failure predictions of short fiber thermoplastic composites.


Degree Type

  • Doctor of Philosophy


  • Aeronautics and Astronautics

Campus location

  • West Lafayette

Advisor/Supervisor/Committee Chair

Dr. Michael D. Sangid

Additional Committee Member 2

Dr. Chelsea Davis

Additional Committee Member 3

Dr. Tyler Tallman

Additional Committee Member 4

Dr. Charles L. Tucker III

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